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HRID11043

反应详情

EQUATION

反应方程式

HRID 11043 的结构方程式

REACTANTS

反应物

2
结构：O=C1C=CC(=O)N1
HCID10935

Maleimide

C4H3NO2

结构：COc1ccc2[nH]c(C=Cc3cc([N+](=O)[O-])cc([N+](=O)[O-])c3)cc2c1
HCID86760190

未命名化合物

PRODUCTS

生成物

1
结构：COc1ccc2[nH]c3c(c2c1)C1C(=O)NC(=O)C1C(c1cc([N+](=O)[O-])cc([N+](=O)[O-])c1)C3
HCID86760189

未命名化合物

收率 89%

PROCEDURE

实验过程

The reaction of 5-Methoxy-2-[2-(3,5-dinitrophenyl)ethenyl]-1H-indole (II; Ar=3,5-dinitrophenyl) (40) prepared as described in example 46 with maleimide using the procedure described in example 69 gave 4-(3,5-Dinitrophenyl)-9-methoxy-4,5,6,10c-tetrahydropyrrolo[3,4-c]carbazole-1,3(2H,3aH)-dione (IV; Ar=3,5-dinitrophenyl, R10═H) (41) in a 89% yield as a glassy solid which was used without further purification.

WORKUP

后处理

  1. customprepared