Acetyl bromide → N-Formyl-2-(4-acetylphenyl)-1,1-dimethylethanamine

Participants

Role	Name	HCID	Charge
Reactant	Acetyl bromide	HCID 10482	—
Reactant	N-(1,1-Dimethyl-2-phenylethyl)formamide	HCID 104077	—
Reactant	Aluminum(III) Chloride	HCID 6451240	—
Solvent	1,2-Dichloroethane	HCID 11	—
Product	N-Formyl-2-(4-acetylphenyl)-1,1-dimethylethanamine	HCID 20556097	—

Reaction Steps

This was prepared in an identical manner to the compound described in Description 10 using aluminum chloride (26 g), acetyl bromide (115 ml) and N-formyl-2-phenyl-1, 1-dimethylethanamine (101.5 g) in 1,2-dichloroethane, (850 ml). τ(CDCl3). 8.62 (6H, s), 7.45 (3H, s), 7.1+6.85 (2H, s+s), 3.85 (1H, broad) 2.7 (2H, d, J=8 Hz) 2.1 (2H, d, J=8 Hz), 1.9 (1H, s).

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US04309443
Source dataset	uspto-grants-1982_01
ORD ID	ord-c216a8b6494248a882b98526218a7ea6
Source note	uspto-grants-1982_01