HRID1105635

反应详情

EQUATION

反应方程式

HRID 1105635 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

This was prepared in an identical manner to the compound described in Description 10 using aluminum chloride (26 g), acetyl bromide (115 ml) and N-formyl-2-phenyl-1, 1-dimethylethanamine (101.5 g) in 1,2-dichloroethane, (850 ml). τ(CDCl3). 8.62 (6H, s), 7.45 (3H, s), 7.1+6.85 (2H, s+s), 3.85 (1H, broad) 2.7 (2H, d, J=8 Hz) 2.1 (2H, d, J=8 Hz), 1.9 (1H, s).

WORKUP

后处理

  1. customThis was prepared in an identical manner to the compound