HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisopropylamine → 11alpha,15-Dihydroxy-15-methyl-9-oxo-13-thia-5-prostenoic acid p-benzoylaminophenyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisopropylamine | HCID 7912 | — |
| Reactant | 2-Methyl-1-sulfanylheptan-2-OL | HCID 13506860 | — |
| Reactant | 7-(3-Hydroxy-5-oxo-1-cyclopenten-1-yl)-hept-5-enoic acid p-benzoylaminophenyl ester | HCID 57189790 | — |
| Product | 11alpha,15-Dihydroxy-15-methyl-9-oxo-13-thia-5-prostenoic acid p-benzoylaminophenyl ester | HCID 70554139 | — |
Reaction Steps
Analogously to Example 5, by reaction of 7-(3-hydroxy-5-oxo-1-cyclopenten-1-yl)-hept-5-enoic acid p-benzoylaminophenyl ester with 2-hydroxy-2-methyl-heptanethiol in the presence of diisopropylamine, 11α,15-dihydroxy-15-methyl-9-oxo-13-thia-5-prostenoic acid p-benzoylaminophenyl ester is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04309441 |
| Source dataset | uspto-grants-1982_01 |
| ORD ID | ord-8b11e128573846898c3a0c8113c8a24b |
| Source note | uspto-grants-1982_01 |