HRID1105647
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
A mixture of 9 g. of 5-bromopentanoic acid, 10.2 g. of dicyclohexyl carbodiimide and 10.75 g. of p-benzoylaminophenol was boiled for 2 hours in benzene. After cooling, the solution was filtered and the solvent distilled off. As a residue 5-bromopentanoic acid p-benzoylaminophenyl ester was obtained.
WORKUP
后处理
- additionA mixture of 9 g
- temperatureAfter cooling
- filtrationthe solution was filtered
- distillationthe solvent distilled off