HRID1105647

反应详情

EQUATION

反应方程式

HRID 1105647 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A mixture of 9 g. of 5-bromopentanoic acid, 10.2 g. of dicyclohexyl carbodiimide and 10.75 g. of p-benzoylaminophenol was boiled for 2 hours in benzene. After cooling, the solution was filtered and the solvent distilled off. As a residue 5-bromopentanoic acid p-benzoylaminophenyl ester was obtained.

WORKUP

后处理

  1. additionA mixture of 9 g
  2. temperatureAfter cooling
  3. filtrationthe solution was filtered
  4. distillationthe solvent distilled off