HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dicyclohexylcarbodiimide → 5-Bromopentanoic acid p-benzoylaminophenyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dicyclohexylcarbodiimide | HCID 10868 | — |
| Reactant | 5-Bromovaleric acid | HCID 16368 | — |
| Reactant | Benzamide, N-(4-hydroxyphenyl)- | HCID 459327 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | 5-Bromopentanoic acid p-benzoylaminophenyl ester | HCID 54396007 | — |
Reaction Steps
A mixture of 9 g. of 5-bromopentanoic acid, 10.2 g. of dicyclohexyl carbodiimide and 10.75 g. of p-benzoylaminophenol was boiled for 2 hours in benzene. After cooling, the solution was filtered and the solvent distilled off. As a residue 5-bromopentanoic acid p-benzoylaminophenyl ester was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04309441 |
| Source dataset | uspto-grants-1982_01 |
| ORD ID | ord-1d33917e1e7f43d980742e3e40424eeb |
| Source note | uspto-grants-1982_01 |