Water → HCID 73683446, compound

HRID 1105704Notes

Reaction equation

HRID 1105704 reaction equation
[CH2:1]([NH:17][C:18]1[CH:25]=[CH:24][C:21]([CH:22]=O)=[CH:20][CH:19]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16].[OH2:26].Cl.[NH2:28]O>C(O)C.C(O)(=O)C>[CH2:1]([NH:17][C:18]1[CH:25]=[CH:24][C:21]([CH:22]=[N:28][OH:26])=[CH:20][CH:19]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16]

Participants

5

Reactant 3

HCID 962WaterHCID 443297Hydroxyamine hydrochlorideHCID 13019276HCID 13019276, compound

Product 1

HCID 73683446HCID 73683446, compound

Reagents, catalysts & solvents 1

HCID 18476134Acetic acid ethanolSolvent

Procedure

p-Hexadecylaminobenzaldehyde in ethanol-acetic acid is treated with a concentrated water solution of hydroxylamine hydrochloride. The solid is collected after a brief period, washed with alcohol, and dried to provide the product of the Example.

Workup

  1. customThe solid is collected after a brief period
  2. washwashed with alcohol
  3. customdried
  4. customto provide the product of the Example

Sources & evidence

ORD record
ord-dd7602b3ba154fecaf470933b089f1f0
Source dataset
uspto-grants-1982_01
Patent number
US04309553

Reaction notes

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