HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrafluoroboric acid → Iodonium, diphenyl-, hexafluorophosphate(1-) (1:1)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrafluoroboric acid | HCID 28118 | — |
| Reactant | Diphenyliodonium chloride | HCID 73870 | — |
| Reactant | Hexafluorophosphoric acid | HCID 16211447 | — |
| Product | Iodonium, diphenyl-, hexafluorophosphate(1-) (1:1) | HCID 2737136 | 74% |
Reaction Steps
The procedure of Example 1 was repeated for preparing an aromatic halonium salt using diphenyliodonium chloride. In this preparation, fluoroboric acid was replaced by 25 ml (60%) hexafluorophosphoric acid. There was obtained a 74% yield of diphenyliodonium hexafluorophosphate having a m.p. of 139°-141° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04310469 |
| Source dataset | uspto-grants-1982_01 |
| ORD ID | ord-48642f58e3b84aca8818938e77021646 |
| Source note | uspto-grants-1982_01 |