HRID1105977

反应详情

EQUATION

反应方程式

HRID 1105977 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

23.0 g of 2-acetylamino-4-t-butyl-5-hexadecyloxyphenol obtained in Example 1, 120 ml of ethanol and 96 ml of 35% hydrochloric acid were blended, and the mixture was refluxed for 5 hours with stirring. After cooling the reaction solution, the crystals formed were separated by filtration to obtain 23.2 g of 2-amino-4-t-butyl-5-hexadecyloxyphenol hydrochloride.

WORKUP

后处理

  1. temperaturethe mixture was refluxed for 5 hours
  2. temperatureAfter cooling the reaction solution
  3. customthe crystals formed
  4. customwere separated by filtration