Dichloroacetyl chloride → HCID 20554040, compound

HRID 1105996Notes

Reaction equation

C(N)C#C.ClC=CC(Cl)Cl.[CH2:11]([NH:14][CH2:15][CH:16]=[C:17]([Cl:19])[Cl:18])[C:12]#[CH:13].[Cl:20][CH:21]([Cl:25])[C:22](Cl)=[O:23]>>[CH2:11]([N:14]([CH2:15][CH:16]=[C:17]([Cl:19])[Cl:18])[C:22](=[O:23])[CH:21]([Cl:25])[Cl:20])[C:12]#[CH:13]

Participants

Reactant 4

HCID 6593Dichloroacetyl chloride

HCID 1178191-Propene, 1,3,3-trichloro-

HCID 239041Propargylamine

HCID 20554026HCID 20554026, compound

Product 1

HCID 20554040HCID 20554040, compound

Procedure

From propargylamine and 1,3,3-trichloropropene, proceeding as in Example 1, there was prepared N-propargyl-N-(3,3-dichloroallyl)amine: b.p.15 mm =88°-91° C., from which, by reaction with dichloroacetyl chloride, there was obtained N-propargyl-N-(3,3-dichloroallyl)dichloroacetamide, (Applicants' Mark 8341), a yellowish oil.

Sources & evidence

ORD record: ord-d007f753cbdf489eba2e03c8fe938ed4
Source dataset: uspto-grants-1982_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04311516

Reaction notes

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