HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diazomethane → HCID 14036305, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diazomethane | HCID 9550 | — |
| Reactant | HCID 12821144 | HCID 12821144 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 14036305 | HCID 14036305 | — |
Reaction Steps
A solution of the product from Example 3 in ether is treated with a slight excess of diazomethane. After standing at room temperature, the solvent is evaporated to give (S)-1-[3-(acetylthio)-2-methyl-1-oxopropyl]-4,4-dimethoxy-L-proline, methyl ester.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04311697 |
| Source dataset | uspto-grants-1982_01 |
| ORD ID | ord-dd0eaf28330e4cad9a3a0e508592fd54 |
| Source note | uspto-grants-1982_01 |