HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Hydroxybenzaldehyde → HCID 136025196, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Hydroxybenzaldehyde | HCID 126 | — |
| Reactant | Sodium Chloride | HCID 5234 | — |
| Reactant | 1H-Pyrazole-3-carboxamide, 4,5-dihydro-5-oxo-1-phenyl- | HCID 80813 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 136025196 | HCID 136025196 | — |
Reaction Steps
20.5 g (0.1 mole) of 1-phenyl-3-carbamoyl-2-pyrazolin-5-one and 12.2 g (0.1 mole) of p-hydroxybenzaldehyde were stirred for 1 hour in 100 ml of boiling dimethylformamide. The hot reaction mixture was poured out in 500 ml of an aqueous solution of sodium chloride (12%). After stirring and standing for a while, the yellow dye was filtered with suction, rinsed with water, and washed with hot acetone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04311787 |
| Source dataset | uspto-grants-1982_01 |
| ORD ID | ord-80ddd21c63314ee693a17d935229acc0 |
| Source note | uspto-grants-1982_01 |