Citric Acid → HCID 131712651, compound

HRID 1106198Notes

Reaction equation

HRID 1106198 reaction equation
[CH2:1](I)[CH3:2].[OH-].[C:5]([OH:17])(=[O:16])[CH2:6][C:7]([CH2:12][C:13]([OH:15])=[O:14])([C:9]([OH:11])=[O:10])[OH:8].[N:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1>>[C:5]([O-:17])(=[O:16])[CH2:6][C:7]([CH2:12][C:13]([O-:15])=[O:14])([C:9]([O-:11])=[O:10])[OH:8].[CH2:23]([N+:18]1[CH:2]=[CH:1][CH:21]=[CH:20][CH:19]=1)[CH3:22].[CH2:23]([N+:18]1[CH:2]=[CH:1][CH:21]=[CH:20][CH:19]=1)[CH3:22].[CH2:23]([N+:18]1[CH:2]=[CH:1][CH:21]=[CH:20][CH:19]=1)[CH3:22]

Participants

5

Procedure

Pyridine is reacted with ethyl iodide; the halide intermediate is converted to the hydroxide with Rexyn 201 (Fisher Scientific Co.), and then reacted with citric acid.

Sources & evidence

ORD record
ord-6837f1833b4f457d87607ffa64951d3b
Source dataset
uspto-grants-1982_01
Patent number
US04312367

Reaction notes

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