HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 18788736, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 4-Bromo-2-methyl-5-nitrobenzoic acid | HCID 18788890 | — |
| Product | HCID 18788736 | HCID 18788736 | — |
Reaction Steps
14.3 g of 4-bromo-2-methyl-5-nitrobenzoic acid were dissolved in 250 ml of MeOH and 11.6 g of SOCl2 were slowly added dropwise. The mixture was allowed to stand at RT for 5 days, the volatile components were removed in vacuo and the residue is recrystallized from DIP.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06057322 |
| Source dataset | uspto-grants-2000_05 |
| ORD ID | ord-389bcea3dda7445699161a224c184978 |
| Source note | uspto-grants-2000_05 |