HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 70186531, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 9927305 | HCID 9927305 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 70186531 | HCID 70186531 | 100% |
Reaction Steps
To a solution of (S)-4-[α-(hydroxymethyl)benzylamino]-6,7dimethoxyquinazoline (325 mg, 1 mmol) in ethanol (2 ml) was added 1N hydrochloric acid (2 ml, 2 mmol) and the resulting mixture was evaporated under vacuum to dryness to give pure title compound in about 100% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06057326 |
| Source dataset | uspto-grants-2000_05 |
| ORD ID | ord-495a125c252d404ca409fa930b041a87 |
| Source note | uspto-grants-2000_05 |