HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18789323, compound → HCID 18789350, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18789323 | HCID 18789323 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 18789350 | HCID 18789350 | 98.6% |
Reaction Steps
3-(2-Indanyl)carbonylamino-5-(4-vinylphenyl)pyrazole (25.0 mg) was dissolved in ethanol (5.0 ml) to which was subsequently added 10% palladium-carbon (22 mg), and then the mixture was stirred under hydrogen atmosphere of 1 atmospheric pressure overnight. The catalyst was filtered off and then, the filtrate was concentrated under a reduced pressure to obtain the title compound (24.8 mg) as colorless crystals (melting point: 196-198° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06057335 |
| Source dataset | uspto-grants-2000_05 |
| ORD ID | ord-6e0b719998c041ccabfd7747b02521a8 |
| Source note | uspto-grants-2000_05 |