Hydrogen chloride-ethyl acetate → HCID 86755374, compound

Participants

Reaction Steps

4N Hydrochloric acid/ethyl acetate solution (0.20 ml) was added to a solution of N-[3-(dimethylamino)propyl]-[2-(1-octadecanoyl-2-piperidyl)ethoxy]formamide (0.200 g) in ethyl acetate (2 ml). After being stirred for 15 minutes at room temperature, the reaction mixture was concentrated. The residue was recrystallized with ethyl acetate, thereby yielding the entitled compound (0.183 g) as white crystals.

Provenance & Evidence