Hydrogen chloride-ethyl acetate → HCID 86755375, compound

HRID 1106666Notes

Reaction equation

HRID 1106666 reaction equation
[ClH:1].C(OCC)(=O)C.[O:8]1[CH2:13][CH2:12][N:11]([CH2:14][CH2:15][CH2:16][N:17]([O:20][CH2:21][CH2:22][CH:23]2[CH2:28][CH2:27][CH2:26][CH2:25][N:24]2[C:29](=[O:47])[CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][CH2:39][CH2:40][CH2:41][CH2:42][CH2:43][CH2:44][CH2:45][CH3:46])[CH:18]=[O:19])[CH2:10][CH2:9]1>C(OCC)(=O)C>[ClH:1].[O:8]1[CH2:13][CH2:12][N:11]([CH2:14][CH2:15][CH2:16][N:17]([O:20][CH2:21][CH2:22][CH:23]2[CH2:28][CH2:27][CH2:26][CH2:25][N:24]2[C:29](=[O:47])[CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][CH2:39][CH2:40][CH2:41][CH2:42][CH2:43][CH2:44][CH2:45][CH3:46])[CH:18]=[O:19])[CH2:10][CH2:9]1

Participants

4

Reactant 2

HCID 21866389Hydrogen chloride-ethyl acetateHCID 57009431HCID 57009431, compound

Product 1

HCID 86755375HCID 86755375, compound

Reagents, catalysts & solvents 1

HCID 8857Ethyl AcetateSolvent

Procedure

4N Hydrochloric acid/ethyl acetate solution (0.26 ml) was added to a solution of N-(3-morpholinopropyl)-[2-(1-octadecanoyl-2-piperidyl)ethoxy]formamide (0.500 g) in ethyl acetate (5 ml). After being stirred for 15 minutes at room temperature, the reaction mixture was concentrated, thereby yielding the entitled compound (0.532 g) as white solid.

Workup

  1. concentrationthe reaction mixture was concentrated

Sources & evidence

ORD record
ord-51e67af559b742c2a62f919176aef99d
Source dataset
uspto-grants-2000_05
Patent number
US06057337

Reaction notes

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