Hydrogen chloride-ethyl acetate → HCID 86755377, compound

Participants

Reaction Steps

4N Hydrochloric acid/ethyl acetate solution (0.58 ml) was added to a solution of N-[3-(dimethylamino)propyl]-[2-(1-docosanoyl-2-piperidyl)ethoxy]formamide (1.04 g) in ethyl acetate (11 ml) at room temperature. After being stirred for 20 minutes, the reaction mixture was concentrated. The residue was recrystallized with ethyl acetate, thereby yielding the entitled compound (1.12 g) as white crystals.

Provenance & Evidence