HCID 15897853, compound → HCID 15897852, compound

Participants

Reaction Steps

4N Hydrochloric acid/ethyl acetate solution (1.34 ml) was added to a solution of 2-(1-docosanoyl-2-piperidyl)ethyl N-[2-(dimethylamino)ethyl]carbamate (2.500 g) in ethyl acetate (25 ml) and the mixture was stirred for 0.5 hour. After the reaction mixture was concentrated, the residue was recrystallized with a mixed solution of ethyl acetate-ethanol, thereby yielding the entitled compound (2.287 g) as white solid.

Provenance & Evidence