HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 9830126, compound → HCID 70103054, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 9830126 | HCID 9830126 | — |
| Reactant | Hydrogen chloride-ethyl acetate | HCID 21866389 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 70103054 | HCID 70103054 | — |
Reaction Steps
4N Hydrochloric acid/ethyl acetate solution (1.24 ml) was added to a solution of 2-(1-octadecanoyl-2-piperidyl)ethyl 4-benzyltetrahydro- 1 (2H)-pyrazinecarboxylate (2.465 g) in ethyl acetate (25 ml). After being stirred for 30 minutes, the reaction mixture was concentrated. The residue was recrystallized with ethyl acetate, thereby yielding the entitled compound (2.041 g) as white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06057337 |
| Source dataset | uspto-grants-2000_05 |
| ORD ID | ord-9bc18a9073ae46f4a5d94ea02ec84c1b |
| Source note | uspto-grants-2000_05 |