HCID 15897855, compound → HCID 15897856, compound

Participants

Reaction Steps

4N Hydrochloric acid/ethyl acetate solution (1.46 ml) was added to a solution of 2-(1-docosanoyl-2-piperidyl)ethyl 4-methyltetrahydro-1(2H)-pyrazinecarboxylate (2.800 g) in ethyl acetate (28 ml), while being cooled with ice. The mixture was stirred for 30 minutes. After the reaction mixture was concentrated, the residue was recrystallized with ethyl acetate, thereby yielding the entitled compound (2.590 g) as white solid.

Provenance & Evidence