HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 53665391, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 1-Bromo-4-chlorobutane | HCID 81364 | — |
| Reactant | HCID 18789396 | HCID 18789396 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 53665391 | HCID 53665391 | — |
Reaction Steps
Sodium hydride is added to tetrahydrofuran solution of octadecyl 2-(2-hydroxyethyl)piperidinecarboxylate and the mixture is reacted at 0° C. Then, 1-bromo-4-chlorobutane is added to the reaction mixture and reacted to obtain octadecyl 2-(4-chlorobutoxyethyl)piperidinecarboxylate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06057337 |
| Source dataset | uspto-grants-2000_05 |
| ORD ID | ord-28601a97ae6a4c399d4c5e6a2653298c |
| Source note | uspto-grants-2000_05 |