HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → 4-[2-Benzyloxybenzylthio]benzoylchloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | 4-[2-Benzyloxybenzylthio]benzoic acid | HCID 22675551 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 4-[2-Benzyloxybenzylthio]benzoylchloride | HCID 22675537 | — |
Reaction Steps
4-[2-benzyloxybenzylthio]benzoic acid (6.3 g) and oxalyl chloride (2.26 g) were stirred in dichloromethane (100 ml) for 18 hours. The solvent was evaporated to give 4-[2-benzyloxybenzylthio]benzoylchloride which was dissolved in dichloromethane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06057345 |
| Source dataset | uspto-grants-2000_05 |
| ORD ID | ord-5305b701737c40a39f385dff58cce21b |
| Source note | uspto-grants-2000_05 |