HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54451565, compound → HCID 54152782, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54451565 | HCID 54451565 | — |
| Catalyst | Palladium hydroxide | HCID 9942167 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 54152782 | HCID 54152782 | — |
Reaction Steps
To a solution of Example 20 (1.79 g, 3.5 mmol) in ethanol (85 mL) was added palladium hydroxide (20% on carbon) (0.15 g). This was hydrogenated at 30° C. for 6 hours, filtered through Celite, and the solvent removed in vacuo to give a white foam, 3.4 mmol, 96%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06057357 |
| Source dataset | uspto-grants-2000_05 |
| ORD ID | ord-5884ddf4adf742b78b6b8a44f4c352ea |
| Source note | uspto-grants-2000_05 |