HCID 70298427, compound → HCID 70298102, compound

Participants

Reaction Steps

A solution of Example 24 (3.00 g, 5.01 mmol) in absolute ethanol (50 mL) with palladium on charcoal (0.34 g) was hydrogenated at 30° C. and 50 psi for 5.5 hours. The catalyst was removed by filtration through Celite and the filtrate concentrated in vacuo to give the product, 2.195 g. This was used without further purification.

Provenance & Evidence