HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 77332212, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | HCID 70298692 | HCID 70298692 | — |
| Catalyst | Palladium hydroxide | HCID 9942167 | — |
| Product | HCID 77332212 | HCID 77332212 | — |
Reaction Steps
To a solution of Example 39 (2.41 g, 3.8 mmol) in ethanol (220 mL) was added palladium hydroxide (20% on carbon) (0.15 g). This was hydrogenated at 30° C. for 16 hours, filtered through Celite, and the solvent removed in vacuo to give a white foam, 3.7 mmol, 97%. This was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06057357 |
| Source dataset | uspto-grants-2000_05 |
| ORD ID | ord-66436e4c9e714e2096b295b59487a1e6 |
| Source note | uspto-grants-2000_05 |