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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1106915Generated: October 31, 2026

HCID 11015313, compound → HCID 18788111, compound

https://huagongshe.com/reaction/1106915

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 11015313HCID 11015313—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 18788111HCID 18788111—

Reaction Steps

2-Benzyloxycarbonyl-9-tert-butyloxycarbonylmethyl-1,2,3,4-tetrahydro-9H-pyrido-[3,4-b]indole (3.28 g, 7.81 mmol) was stirred under an atmosphere of hydrogen in the presence of 10% palladium on charcoal (500 mg) in methanol (30 ml) at room temperature for two hours. The reaction mixture was filtered through a pad of celite and evaporated to dryness affording the product. (2.14 g, 96%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06057311
Source datasetuspto-grants-2000_05
ORD IDord-7e05433fc5c249d898fbeaa1ca8ff2df
Source noteuspto-grants-2000_05