HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 11015313, compound → HCID 18788111, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 11015313 | HCID 11015313 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 18788111 | HCID 18788111 | — |
Reaction Steps
2-Benzyloxycarbonyl-9-tert-butyloxycarbonylmethyl-1,2,3,4-tetrahydro-9H-pyrido-[3,4-b]indole (3.28 g, 7.81 mmol) was stirred under an atmosphere of hydrogen in the presence of 10% palladium on charcoal (500 mg) in methanol (30 ml) at room temperature for two hours. The reaction mixture was filtered through a pad of celite and evaporated to dryness affording the product. (2.14 g, 96%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06057311 |
| Source dataset | uspto-grants-2000_05 |
| ORD ID | ord-7e05433fc5c249d898fbeaa1ca8ff2df |
| Source note | uspto-grants-2000_05 |