HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 18790157, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 18790170 | HCID 18790170 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 18790157 | HCID 18790157 | — |
Reaction Steps
To a solution of t-butyl 7-phenyl-3-phenylsulfanylheptanoate (1.8 g; 6.5 mmol) in CH2Cl2 (20 mL) is slowly added trifluoroacetic acid (6 mL). The reaction is stirred 5 hours and concentrated in vacuo to yield 7-phenyl-3-phenylsulfanylheptanoic acid which is used directly in Step I.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06057369 |
| Source dataset | uspto-grants-2000_05 |
| ORD ID | ord-6aadaadfb1784da3a7eb4ae8dc9f481f |
| Source note | uspto-grants-2000_05 |