HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,2-Diphenylethylamine → HCID 22444194, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,2-Diphenylethylamine | HCID 77575 | — |
| Reactant | 1-Chloro-2-isothiocyanatobenzene | HCID 123171 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 22444194 | HCID 22444194 | — |
Reaction Steps
The compound was prepared substantially in accordance with the procedure detailed in Example 1, using 2,2-diphenylethylamine (1.61 g, 8.1 mmol) and 2-chlorophenyl isothiocyanate (1.1 ml, 8.2 mmol) in 30 ml of DMF. The crude material was purified by recrystallization (hexanes/EtOAc).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06060484 |
| Source dataset | uspto-grants-2000_05 |
| ORD ID | ord-1b7391721ffb4afaa7278770dfd99280 |
| Source note | uspto-grants-2000_05 |