Cyanogen Bromide → HCID 18787241, compound

HRID 1107429Notes

Reaction equation

HRID 1107429 reaction equation
[C:1]1([CH:7]([C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)[CH2:8][NH2:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[N:16]#[C:17]Br>CCOCC>[C:10]1([CH:7]([C:1]2[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=2)[CH2:8][NH:9][C:17]#[N:16])[CH:11]=[CH:12][CH:13]=[CH:14][CH:15]=1

Participants

4

Reactant 2

HCID 10476Cyanogen BromideHCID 775752,2-Diphenylethylamine

Product 1

HCID 18787241HCID 18787241, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent2×

Procedure

A cold (0° C.) solution of 2,2-diphenylethylamine (3.36 g, 17.0 mmol) in 50 ml of Et2O, was treated with a solution of cyanogen bromide (1.15 g, 10.9 mmol) in 10 ml of Et2O, under N2, resulting in the formation of a white precipitate. This precipitate was removed by filtration and the filtrate was concentrated in vacuo.

Workup

  1. customresulting in the formation of a white precipitate
  2. customThis precipitate was removed by filtration
  3. concentrationthe filtrate was concentrated in vacuo

Sources & evidence

ORD record
ord-f86854424db6432796f5a9f0776bab9f
Source dataset
uspto-grants-2000_05
Patent number
US06060484

Reaction notes

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