HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyanogen Bromide → HCID 18787241, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyanogen Bromide | HCID 10476 | — |
| Reactant | 2,2-Diphenylethylamine | HCID 77575 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 18787241 | HCID 18787241 | — |
Reaction Steps
A cold (0° C.) solution of 2,2-diphenylethylamine (3.36 g, 17.0 mmol) in 50 ml of Et2O, was treated with a solution of cyanogen bromide (1.15 g, 10.9 mmol) in 10 ml of Et2O, under N2, resulting in the formation of a white precipitate. This precipitate was removed by filtration and the filtrate was concentrated in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06060484 |
| Source dataset | uspto-grants-2000_05 |
| ORD ID | ord-f86854424db6432796f5a9f0776bab9f |
| Source note | uspto-grants-2000_05 |