HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → 2-Ethylphenyl isocyanate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 2-Ethylaniline | HCID 11357 | — |
| Reactant | Triphosgene | HCID 94429 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 2-Ethylphenyl isocyanate | HCID 583486 | — |
Reaction Steps
The compound was prepared substantially in accordance with the procedure detailed in Example 27A, using 2-ethylaniline (1.5 ml, 12.2 mmol), Et3N (4.3 ml, 30.4 mmol) and triphosgene (1.2 g, 4.0 mmol) in 45 ml of CH2Cl2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06060484 |
| Source dataset | uspto-grants-2000_05 |
| ORD ID | ord-c7c70eca27844f6c928a46b5928c8106 |
| Source note | uspto-grants-2000_05 |