Hydrochloric Acid → HCID 18787506, compound

Participants

Reaction Steps

0.2 g (0.81 mmol) of 2,3-dimethyl-7-[l-(diethylamino)ethyl]benzofuran and 2 ml of a 6N solution of hydrochloric acid in isopropanol are placed in a 100 ml round-bottomed flask. The salt is concentrated under vacuum and recrystallized from ethyl acetate and diisopropyl ether. 0.142 g (Yield: 61%) of 2,3-dimethyl-7-[1-(diethylamino)ethyl]benzofuran hydrochloride is obtained in the form of a solid. M.p.=28-30° C.

Provenance & Evidence