Ethanethiol → HCID 23512909, compound

Participants

Reaction Steps

6-Methoxy-2-(4-methoxyphenyl)-3-(4-[(1-methylpiperidin-2-yl)methoxy]benzoyl)benzo[b]thiophene (339 mg, 0.676 mmol), ethane thiol (8.75 mmol), and aluminum chloride (541 mg, 4.06 mmol) were converted to 195 mg (61%) of the title compound by the procedure of Example 16. MS(FD) 473(M+). IR (CHCl3) ν max 3414, 3179, 1605, 1468, 1261, 1170.

Provenance & Evidence