HRID1107587

反应详情

EQUATION

反应方程式

HRID 1107587 的结构方程式

PROCEDURE

实验过程

6-Methoxy-2-(4-methoxyphenyl)-3-(4-[1-benzylpyrrolidin-3-oxy]benzoyl)benzo[b]thiophene (1.57 g, 2.86 mmol), ethane thiol (14.3 mmol), and aluminum chloride (2.29 g, 17.2 mmol) were converted to 566 mg (38%) of the title compound by the procedure of Example 16. MS(FD) 521(M+). IR (CHCl3) ν max 3300, 3027, 3012, 2981, 1732, 1599, 1469, 1257, 1167.