HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanethiol → HCID 12992508, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanethiol | HCID 6343 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Reactant | HCID 9870649 | HCID 9870649 | — |
| Product | HCID 12992508 | HCID 12992508 | 54% |
Reaction Steps
6-Methoxy-2-(4-methoxyphenyl)-3-(4-[(1-methylpiperidin-3-yl)methoxy]benzoyl)benzo[b]thiophene (878 mg, 1.75 mmol), ethane thiol (8.75 mmol), and aluminum chloride (1.40 g, 10.S mmol) were converted to 447 mg (54%) of the title compound by the procedure of Example 16. MS(FD) 473(M+). IR (CHCl3) ν max 3205, 2954, 1599, 1467, 1266, 1171.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06060488 |
| Source dataset | uspto-grants-2000_05 |
| ORD ID | ord-0ef6ae30be59453aa48c25f52a7b936e |
| Source note | uspto-grants-2000_05 |