HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanethiol → HCID 18787302, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanethiol | HCID 6343 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Reactant | HCID 9957112 | HCID 9957112 | — |
| Product | HCID 18787302 | HCID 18787302 | 72.2% |
Reaction Steps
6-Methoxy-2-(4-methoxyphenyl)-3-(4-[1-methylpiperidin-3-oxy]benzoyl)benzo[b]thiophene (310 mg, 0.636 mmol), ethane thiol (3.18 mmol), and aluminum chloride (508 mg, 3.81 mmol) were converted to 211 mg (72%) of the title compound by the procedure of Example 16. MS(FD) 460(M+). IR (CHCl3) ν max 3400, 3149, 2947, 1598, 1467, 1254, 1164.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06060488 |
| Source dataset | uspto-grants-2000_05 |
| ORD ID | ord-134a53b63d2041e2aad864aaf002f391 |
| Source note | uspto-grants-2000_05 |