HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanethiol → HCID 18787292, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanethiol | HCID 6343 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Reactant | HCID 18787305 | HCID 18787305 | — |
| Product | HCID 18787292 | HCID 18787292 | 90% |
Reaction Steps
6-Methoxy-2-(4-methoxyphenyl)-3-(4-[2-ethylpiperidin-3-oxy]benzoyl)benzo[b]thiophene (226 mg, 0.451 mmol), ethane thiol (2.25 mmol), and aluminum chloride (360 mg, 2.70 mmol) were converted to 192 mg (90%) of the title compound by the procedure of Example 16. MS(FD) 474(M+). IR (CHCl3) ν max 3380, 2970, 1597, 1467, 1255, 1165.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06060488 |
| Source dataset | uspto-grants-2000_05 |
| ORD ID | ord-e7ab845db0774bd19f202d560ba08c8e |
| Source note | uspto-grants-2000_05 |