HRID1107591

反应详情

EQUATION

反应方程式

HRID 1107591 的结构方程式

PROCEDURE

实验过程

6-Methoxy-2-(4-methoxyphenyl)-3-(4-[2-pyrrolidin-1-ylcyclohexoxy]benzoyl)benzo[b]thiophene (610 mg, 1.10 mmol), ethane thiol (5.50 mmol), and aluminum chloride (880 mg, 6.60 mmol) were converted to 523 mg (90%) of the title compound by the procedure of Example 16. MS(FD) 528(M+). IR (CHCl3) ν max 3377, 2934, 2857, 1595, 1467, 1258, 1164.