Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Carbon Dioxide | HCID 280 | — |
| Reactant | Ethanol | HCID 702 | — |
| Reactant | (2R,3S,4S,5R,6R)-2-(hydroxymethyl)-6-[(2R,3S,4R,5R,6R)-4,5,6-trihydroxy-2-(hydroxymethyl)oxan-3-yl]oxyoxane-3,4,5-triol;hydrate | HCID 2723821 | — |
| Solvent | Water | HCID 962 | — |
| Product | beta-Maltose | HCID 6255 | — |
Reaction Steps
1.01 g of maltose monohydrate (Sigma UK) was dissolved in 5 ml of deionized water and introduced into a 32 ml particle formation vessel through the intermediate nozzle passage, at a flow rate of 0.03 ml/min. The vessel was maintained at 250 bar and 70° C. Absolute ethanol was co-introduced into the vessel through the inner nozzle passage, at a rate of 0.4 ml/min, and supercritical CO2 through the outer passage at a rate of 9 ml/min. A free-flowing white powder was collected.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06063138 |
|---|
| Source dataset | uspto-grants-2000_05 |
|---|
| ORD ID | ord-c8983c12be4c447ca411de8b045f4129 |
|---|
| Source note | uspto-grants-2000_05 |
|---|
