反应详情

2,2-Dimethyl-3-octenoic acid is prepared by adding 2,2-dimethyl-3-octene nitrile (1.51 g, 0.01 m) to a solution prepared from 15% NaOH in butanol/H2O (2:3) (30 mL). The reaction mixture is stirred and refluxed for 7 hours, is cooled and made acidic with 10% hydrochloric acid. The reaction mixture is extracted with diet hyl ether and the extract washed with saturated NaCl and dried over MgSO4, filtered and concentrated to give 2,2-dimethyl-3-octenoic acid.

1. custom2,2-Dimethyl-3-octenoic acid is prepared
2. temperaturerefluxed for 7 hours
3. temperatureis cooled
4. extractionThe reaction mixture is extracted with diet hyl ether
5. washthe extract washed with saturated NaCl
6. dry with materialdried over MgSO4
7. filtrationfiltered
8. concentrationconcentrated