HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitrogen → 2,2-Dimethyloctanoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitrogen | HCID 947 | — |
| Reactant | 2,2-Dimethyl-3-octenoic acid | HCID 54196509 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2,2-Dimethyloctanoic acid | HCID 62847 | — |
Reaction Steps
2,2-Dimethyl octanoic acid is prepared by dissolving 2,2-dimethyl-3-octenoic acid (0.20 g, 1.1 mmol) in absolute ethanol blanketed with N2 and 10% palladium on carbon which is then hydrogenated for 6 hours. The catalyst is removed by filtration and the filtrate concentrated under vacuum to give 2,2-dimethyl octanoic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06063793 |
| Source dataset | uspto-grants-2000_05 |
| ORD ID | ord-69857e3d0a504371a5d37ddacd51354a |
| Source note | uspto-grants-2000_05 |