HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Pyridinemethanethiol → 1-(2-Butenyl)-2,3-dimethyl-7-(2-pyridylmethylthio)-pyrrolo[2,3-d]pyridazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Pyridinemethanethiol | HCID 256071 | — |
| Reactant | 1-(2-Butenyl)-7-chloro-2,3-dimethylpyrrolo[2,3-d]pyridazine | HCID 53719624 | — |
| Product | 1-(2-Butenyl)-2,3-dimethyl-7-(2-pyridylmethylthio)-pyrrolo[2,3-d]pyridazine | HCID 53930988 | 64.8% |
Reaction Steps
The title compound (cis/trans=20/80) was prepared as a yellow oil in 64.8% yield in a similar procedure to that described in Example 1 by using 1-(2-butenyl)-7-chloro-2,3-dimethylpyrrolo[2,3-d]pyridazine (cis/trans-22/78) and 2-pyridylmethanethiol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06063782 |
| Source dataset | uspto-grants-2000_05 |
| ORD ID | ord-57299c1656ba4789957b039989f33ab1 |
| Source note | uspto-grants-2000_05 |