Homoallyl bromide → HCID 18785613, compound
Reaction equation
[CH3:1][C:2]1[NH:3][C:4]([C:8](=[O:17])[CH2:9][CH2:10][C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)=[CH:5][C:6]=1[CH3:7].Br[CH2:19][CH2:20][CH:21]=C>>[CH3:1][C:2]1[N:3]([CH2:21][CH:20]=[CH2:19])[C:4]([C:8](=[O:17])[CH2:9][CH2:10][C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)=[CH:5][C:6]=1[CH3:7]Participants
3
Procedure
The title compound was prepared as a yellow oil in 86.6% yield in a similar procedure to that described in Referential Example 97 by using 2,3-dimethyl-5-(3-phenylpropionyl)pyrrole and 3-bromomethyl-1-propene.
Sources & evidence
- ORD record
- ord-a31c142d1fd6418cab836ef1232e7e11
- Source dataset
- uspto-grants-2000_05
- Patent number
- US06063782
Reaction notes
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