HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 54356745, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | HCID 54519923 | HCID 54519923 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 54356745 | HCID 54356745 | — |
Reaction Steps
In one example, the primary amine group of compound B5 can optionally be acylated by contacting B5 with an excess of acetic anhydride in methanol containing a trace of water. Generally, this reaction is conducted at about 25° C. to about 30° C. for about 2 to about 24 hours to provide for 3-acetamidocycloheptyl 1-thio-β-galactopyranoside, C5.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06063769 |
| Source dataset | uspto-grants-2000_05 |
| ORD ID | ord-aaeed0e6bfb94e21b5c3385b5ce6f9ff |
| Source note | uspto-grants-2000_05 |