O-Xylene → 3,4-Dimethylbenzaldehyde

HRID 1107925Notes

Reaction equation

HRID 1107925 reaction equation
ClC([O:4][CH3:5])Cl.[CH3:6][C:7]1[CH:8]=[CH:9][CH:10]=[CH:11][C:12]=1[CH3:13]>>[CH3:6][C:7]1[CH:8]=[C:9]([CH:10]=[CH:11][C:12]=1[CH3:13])[CH:5]=[O:4]

Participants

3

Reactant 2

HCID 7237O-XyleneHCID 21004Methane, dichloromethoxy-

Product 1

HCID 222783,4-Dimethylbenzaldehyde

Procedure

The above reaction of Example 68(A) is repeated except that o-xylene and dichloromethyl methylether are the starting materials. Using the same reaction conditions and techniques, there is obtained 3,4-dimethylbenzaldehyde.

Workup

  1. customThe above reaction of Example 68(A)
  2. customthe same reaction conditions and techniques

Sources & evidence

ORD record
ord-9d0e7b0134324ba898a191218c8899d0
Source dataset
uspto-grants-2000_05
Patent number
US06063818

Reaction notes

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