HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → Methyl alpha-(benzoylamino)-4'-sulfo[1,1'-biphenyl]-4-acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | alpha-(Benzoylamino)-4'-sulfo[1,1'-biphenyl]-4-acetic acid | HCID 18786431 | — |
| Product | Methyl alpha-(benzoylamino)-4'-sulfo[1,1'-biphenyl]-4-acetate | HCID 18786424 | — |
Reaction Steps
To a mixture of 12.46 g (30.31 mmol) of α-(benzoylamino)-4'-sulfo[1,1'-biphenyl]-4-acetic acid in 60 mL of methanol was added 6 g of anhydrous hydrogen chloride. When the addition was complete, the mixture was stirred for 2.5 h. The solvent was removed under reduced pressure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06063932 |
| Source dataset | uspto-grants-2000_05 |
| ORD ID | ord-7b512b7fd6d94082978c5bcb70248df7 |
| Source note | uspto-grants-2000_05 |