HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-bromobutanimide → HCID 54157086, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | HCID 53728357 | HCID 53728357 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 54157086 | HCID 54157086 | 93.4% |
Reaction Steps
Prepared from 7-methoxybenzofuran-2-sulfonic acid dimethylamide (0.82 g) and N-bromosuccinimide (0.57 g) in acetonitrile (50 ml). Purification by column chromatography eluting with 50% ethyl acetate in hexane afforded the desired product as a pale yellow solid (1.0 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06066657 |
| Source dataset | uspto-grants-2000_05 |
| ORD ID | ord-c0d17a9715d141bda5e3114d1bd3d57c |
| Source note | uspto-grants-2000_05 |