HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 18784848, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | HCID 18784861 | HCID 18784861 | — |
| Reactant | Oxolane--water (1/1) | HCID 21881883 | — |
| Catalyst | Dichlorobis(triphenylphosphine)palladium | HCID 6102075 | — |
| Product | HCID 18784848 | HCID 18784848 | — |
Reaction Steps
Prepared from 4-bromo-2-methanesulfonyl-7-methoxybenzofuran (1.64 g), triphenylphosphine (0.49 g), bis(triphenylphosphine)palladium (II) chloride (0.25 g) and triethylamine (7.2 ml) in tetrahydrofuran/water (68 ml/35 ml). The title compound was obtained as a white solid (1.23 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06066657 |
| Source dataset | uspto-grants-2000_05 |
| ORD ID | ord-85061c1143524d71886f6f1652748ae3 |
| Source note | uspto-grants-2000_05 |